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ACCESSORIES FOR ALL SPR Navi INSTRUMENTS

SPR Navi: Electrochemistry flow cell.jpg

SPR sensograms of copper deposition with cyclic voltametry using two different potential scanning rates.

 ELECTROCHEMISTRY FLOW CELL *

  • SPR slide acts as working electrode
  • Two insulated hollow tubes for counter and reference electrodes
  • Slide replacement with easy quick-lock mechanism
  • The whole assembly of the SPR slide can be kept under liquid to avoid contact with air!
  • Top of the cuvette is open for pipeting enabling the change of the analyte!
  • By utilizing the built-in two channel peristaltic pump, a continuous liquid flow through the cuvette can be arranged.

Highlights:

  • EC working electrode: SPR sensor surface (e.g. Au)
  • EC counterelectrode and reference electrode: easily exchangable wire e.g. Pt, Ag/AgCl, and others

Modes:

  • SPR and EC measurements in parallel (increase in accuracy compared to separate measurement set-up)
  • EC used as a stimuli

Why SPR Navi for EC measurements?

SPR Navi is especially useful for metals and other highly absorbing materials, which have a non-linear SPR response, because SPR Navi is based on a Multi-Parametric Surface Plasmon Resonance technique (MP-SPR) and measures the full SPR curve and not just a sensogram

Materials

Suitable for organic, inorganic or hybrid conductors and insulators

Applications (application note AN#120)

  • Characterization of above materials
  • Quality control / monitoring of depositions of above materials
  • Detection of trace metals
 

HIGH-RESISTANCE FLOW CELL *

For special applications handling solvents, we offer a flow cell made of PEEK.

 

GAS FLOW CELL*

For applications handling gas samples, we offer a special flow cell.

 

STANDARD FLOW CELL *

A flow cell supplied with our system is made of Poly(DimethylSiloxane), PDMS. Standard cell volume is 1 µl. Others by request.

Immobilizer for SPR Navi

IMMOBILIZER

Small, stand-alone flow cell, oriented horizontally, with manual pipetting, for in-situ functionalisation of SPR slides.

Note: * All SPR Navi™ flow cells can be easily exchanged by user.

ACCESSORIES FOR SPR Navi 200

 SPR Navi 200 with an external autosampler.

AUTOSAMPLER

 Spark Holland Alias Cool Autosampler  accessory for SPR Navi 200 for high throughput, multi-sample or multi-injection experiments. 

 
General         

  • Easy to operate and maintain       
  • Sample cooling: (Minimum: 4°C ± 2°C, Maximum: ambient temp -3°C)      
  • Biocompatible fluidics (PEEK™ tubing, coated needle) 
  • Dimensions: 300 mm x 575 mm x 360 mm (with cooling)
  • Weight: 21 kg (with cooling) 
  • Max. weight that can be placed on top of autosampler:  65 kg
  • Power requirements: 95 - 240 Volt AC ± 10%; 50 - 60 Hz; 200VA

 

Sampling

  • Sample capacity: 2 microtiter plates, 2x 48 vials (1.5 mL), or 2x 12 vials (10 mL, optional)
  • Loop volume: 1 - 5000 μL programmable, 10 mL loop optional, exchangeable
  • Dispenser syringe: 500 μL standard (250, 1000 and 2500 μL optional)
  • Switching time injection valve: Electrically < 100 msec 
  • Injection cycle time: < 60 sec. in all injection modes for 1 injection <100 μL including 300 μL wash

Analytical performance

  • Injection modes: Full loop, partial loopfill and μL pickup mode, PASA™ (pressure-assisted sample aspiration)
  • Reproducibility: RSD £ 0.3% for full loop injections; RSD ≤0.5% for partial loopfill injections
  • Memory effect: < 0.05% with programmable needle wash

Programming

  • Software integrated with SPR Navi 200
  • Injection methods: Full loop, partial loopfill and μL pickup 
  • Injection volume: 0 μL - 9.999 μL (with 1 μL increment), depending on system settings
  • Analysis time: max. 9 hr, 59 min, 59 sec
  • Wash: Programmable, wash between injections and wash between vials

Communication

  • USB 2.0
  • On request: RS232C, RS422/485, CAN, Ethernet
 

DEGASSER

Prevents air bubble formation. Useful especially in long measurements.

2-channel degasser, internal volume only 480 µl, eliminates baseline fluctuations, advanced error and leak checking functions, wetted parts: PEEK and Systec AF

syringe_pump_for_SPR_Navi.jpg

SYRINGE PUMP

Good for measurements where low flow rate and extreme flow stability are needed. Mainly for biochemical interactions, when the sensor response is low and long interaction time is needed.

2-channel syringe pump, flowrates 0.831 nL/min - 150.5mL/min, syringe sizes 10 L - 140 mL, weight 4.3 kg, control over RS485 or LCD display.